Eyona Ruscogenin CAS No.472-11-7 uMvelisi kunye Factory |Yongjian

Ruscogenin CAS No.472-11-7

Inkcazelo emfutshane:

I-Ruscogenin yinto yekhemikhali ene-molecular formula C27H42O4.

Igama lesiNgesi

(1B,3B,25R)-SPIROST-5-ENE-1,3-DIOL;RUSCOGENIN;RUSCOGENIN;(25R)-spirost-5-ene-1-beta,3-beta-diol;Spirost-5-ene- I-1,3-diol, (1.beta.,3.beta.,25R); RUSCOGENIN (P); (25R) -Spirost-5-ene-1β,3β-diol;

Thumela i-imeyile kuthi

Iinkcukacha zeMveliso

Iithegi zeMveliso

Ulwazi oluBalulekileyo

[Ubunzima beMolekyuli]430.63

[Inombolo yeCAS]472-11-7

[Indlela yokubona]HPLC ≥ 98%

[Iinkcukacha]20mg, 50mg, 100mg, 500mg, 1g (inokupakishwa ngokweemfuno zabathengi)

[Umlinganiswa]Le mveliso iyinaliti emhlophe ye-crystal powder.

[Umsebenzi kunye nokusetyenziswa]Le mveliso isetyenziselwa ukumisela umxholo.

[Umthombo wokutsalwa]Le mveliso yingcambu ye-Ophiopogon japonicus (L · f ·) Ker Gawl.

Iipropati ze-Pharmacological

Ine-anti-inflammatory ebalulekileyo, inciphisa i-capillary permeability, ilawula ukungasebenzi kakuhle kwe-prostate, inhibiting G + ibhaktheriya kunye ne-anti elastase.

Ukumiselwa komxholo

Ukulungiswa kwesisombululo sereferensi:thatha isixa esifanelekileyo sesisombululo sereferensi yeRuscogenin, ulinganise ngokuchanekileyo, kwaye udibanise i-methanol ukuze iqulethe i-50% nge-1ml nganye ye-G isisombululo. ml yesisombululo sereferensi, zibeke kwi-flask ye-conical kunye ne-stopper ngokulandelanayo, kwaye ukhuphe i-solvent kwindawo yokuhlamba amanzi.Yongeza ngokuchanekileyo i-10ml ye-perchloric acid, yigubungele kakuhle, yigcine emanzini atshisayo imizuzu eyi-15, yikhuphe, uyipholise ngamanzi e-ice, thatha i-reagent ehambelanayo njengento engenanto, ukulinganisa ukuxhamla kwi-wavelength ye-397nm ngokuhambelana ne-ultraviolet ebonakalayo spectrophotometry. Isihlomelo VA), thatha i-absorbence njenge-ordination kunye ne-concentration njenge-abscissa, kwaye uzobe i-curve esemgangathweni.

Ukulungiswa kwesisombululo sovavanyo:thatha malunga ne-3G yomgubo ococekileyo wemveliso, uyilinganise ngokuchanekileyo, uyibeke kwi-flask ye-conical ene-stopper, yongeza ngokuchanekileyo i-50ml ye-methanol, ilinganise, ukushisa kunye ne-reflux kwiiyure ze-2, yipholise, ilinganise, yenza ubunzima obulahlekileyo. ngemethanol, yihlube kakuhle kwaye uyihluze.Ukulinganisa ngokuchanekileyo i-25ml ye-filtrate eqhubekayo, yifake kwi-flask, buyisela i-solvent ukuze yome, yongeza i-10ml yamanzi ukunyibilikisa intsalela, ihluthise ngamanzi, ivuthulule nge-n-butanol ngamaxesha ama-5, i-10ml ngexesha ngalinye, udibanise i-n. -isisombululo se-butanol, sihlambe kabini ngesisombululo sovavanyo lwe-ammonia, i-5ml ngexesha ngalinye, ulahle isisombululo se-ammonia, kwaye ukhuphe isisombululo se-n-butanol ukuze some.Chitha intsalela nge-80% ye-methanol kwaye uyidlulisele kwi-flask yevolumetric ye-50ml, yongeza i-80% ye-methanol kwisikali kwaye ugubungele kakuhle.

Indlela yokumisela ngokuchanekileyo ukulinganisa i-2 ~ 5ml yesisombululo sovavanyo, uyibeke kwi-10ml edibeneyo ityhubhu yokuvavanya eyomileyo, ngokwendlela ephantsi kokulungiswa kwegophe eliqhelekileyo, ukulinganisa i-absorbction ngokomthetho ukusuka "ku-volatilizing i-solvent kwi-bath yamanzi", funda inani le-ruscoegenin kwisisombululo sovavanyo ukusuka kwi-curve esemgangathweni kwaye uyibale.

I-saponins iyonke ye-Ophiopogon japonicus ayiyi kuba ngaphantsi kwe-0.12% ngokusekelwe kwi-Ruscogenin (C27H42O4).

Iimeko zeChromatographic: (ngereferensi kuphela)